1158098-73-7
1158098-73-7
Top Quality 1158098-73-7 6704-31-0 Hot Sell In Stock
- Molecular Formula:C3H4O2
- Molecular Weight:72.0636
- Refractive Index:1.426
- Boiling Point:139.7 °C at 760 mmHg
- Flash Point:52.931 °C
- PSA：26.30000
- Density:1.231 g/cm3
- LogP:-0.41430
6704-31-0 Relevant articles
Synthesis method of 3-oxetanone
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Paragraph 0040; 0046-0048; 0054-0056; 0062-0062, (2020/11/25)
The invention discloses a synthesis meth...
A method for synthesis of oxetane butanone (by machine translation)
-
Paragraph 0021; 0022, (2019/03/26)
The present invention provides a method ...
3-oxetanone synthesis method
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Paragraph 0019; 0021, (2019/05/04)
The invention provides a 3-oxetanone syn...
Preparation method for 3-oxetanone
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Paragraph 0050; 0051; 0052; 0053; 0054; 0055; 0056-0064, (2019/01/08)
The invention discloses a preparation me...
6704-31-0 Process route
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7748-36-9
oxetan-3-ol
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-
6704-31-0
oxetan-3-one
| Conditions | Yield |
|---|---|
|
With
phosphorus pentoxide; triethylamine;
In
dichloromethane; dimethyl sulfoxide;
at 10 - 40 ℃;
for 2h;
Solvent;
Reagent/catalyst;
|
65.3% |
|
With
phosphorus pentoxide; dimethyl sulfoxide; triethylamine;
In
dichloromethane;
at -5 - 5 ℃;
|
48% |
|
With
pyridine; chromium(VI) oxide;
In
dichloromethane;
at 5 - 20 ℃;
|
|
|
With
phosphorus pentoxide; dimethyl sulfoxide; triethylamine;
In
dichloromethane;
Large scale;
Industrial scale;
|
|
|
With
9-azabicyclo<3.3.1>nonane-N-oxyl; oxygen; acetic acid; sodium nitrite;
at 20 ℃;
for 2h;
under 760.051 Torr;
Reagent/catalyst;
Solvent;
|
93 %Spectr. |
|
With
N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; sodium hydrogencarbonate;
In
dichloromethane;
at 30 - 40 ℃;
for 2h;
Reagent/catalyst;
|
49.0 g |
-
-
3-chloro-2-oxopropyl-2-bromobenzoate
-
-
6704-31-0
oxetan-3-one
| Conditions | Yield |
|---|---|
|
With
potassium hydroxide;
In
methanol;
at 80 ℃;
for 8h;
Solvent;
Temperature;
Reagent/catalyst;
|
72% |
6704-31-0 Upstream products
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diazomethane
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chloroacetyl chloride
-
922500-97-8
3,3-dimethoxyoxetane
-
7748-36-9
oxetan-3-ol
6704-31-0 Downstream products
-
1020818-00-1
(4-chloro-phenyl)-oxetan-3-yl-amine
-
1085453-63-9
4-(3-hydroxyoxetan-3-yl)benzenecarbonitrile
-
922500-91-2
ethyl 2-(oxetan-3-ylidene)acetate
-
1159599-85-5
3-[6-(5-Methyl-3-phenyl-isoxazol-4-ylmethoxy)-pyridin-3-yl]-oxetan-3-ol
