

|
Flammability and Explosibility |
Nonflammable |
|
Synthesis |
Expose 3 mL of a 0.018 mg/mL solution of 3-diethylaminophenyl 2-hexanoxycarbonylbenzoate in methanol to UV-B radiation in a Luzchem LZC-4 photoreactor equipped with 16 broad band UV-B lamps (LES-UVB-01) at 35 °C to obtain Diethylamino hydroxybenzoyl hexyl benzoate. |
|
in vitro |
Diethylamino hydroxybenzoyl hexyl benzoate (DHHB) absorbs UV-A radiation with a peak at 354 nm. The molar absorption coefficient of Diethylamino hydroxybenzoyl hexyl benzoate in EtOH at 25°C is obtained to be 39 000 mol/dm 3 /cm at 354 nm. The emission spectrum of Diethylamino hydroxybenzoyl hexyl benzoate in EtOH is dependent on the excitation wavelength. |
|
Application |
Hexyl 2-[4-(diethylamino)-2-hydroxybenzoyl]benzoate may be used as a test material in investigating the structural elucidation of its transformation products in chlorinated water using liquid chromatography coupled to mass spectrometry. |
InChI:InChI=1/C24H31NO4/c1-4-7-8-11-16-29-24(28)20-13-10-9-12-19(20)23(27)21-15-14-18(17-22(21)26)25(5-2)6-3/h9-10,12-15,17,26H,4-8,11,16H2,1-3H3
The present invention relates to a metho...
The invention discloses a synthesis meth...
The present invention relates to a compo...
The present invention relates to a metho...

1-Chlorohexane


2'-Carboxy-4-diethylamino-2-hydroxybenzophenon


n-hexyl 2-(4-diethylamino-2-hydroxybenzoyl)benzoate
| Conditions | Yield |
|---|---|
|
With potassium carbonate; In N,N-dimethyl-formamide; at 100 - 110 ℃; for 4h; Large scale;
|
86% |

mono-n-hexyl phthalate


3-diethylaminophenol


n-hexyl 2-(4-diethylamino-2-hydroxybenzoyl)benzoate
| Conditions | Yield |
|---|---|
|
With zinc(II) chloride; trichlorophosphate; In dimethyl sulfoxide; at 20 - 50 ℃; for 5h; Solvent; Temperature;
|
95% |

n-hexyl methanesulfonate

2'-Carboxy-4-diethylamino-2-hydroxybenzophenon

4-methylbenzenesulfonic acid n-hexylester

dihexyl sulfite